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Accession number;03A0275221
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| Title;Effect of Solvent on Extraction-GC/EI-MS Measurement of Pesticides Fixed on Disk-format Solid Phase |
| Author;
KITAHARA TAKIO
(Tokai Univ., School of Science)
TAKANO JIRO
(Tokai Univ., School of Science)
KITAMI HIDEAKI
(Sogokankyobunseki Gijutsubu)
WATANABE TETSUO
(Tokai Univ., Coll. of Gen. Educ.)
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Journal Title;Proc Sch Sci Tokai Univ
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Journal Code:S0439A
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ISSN:0919-5025
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VOL.38;NO.;PAGE.185-194(2003)
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| Figure&Table&Reference;FIG.1, TBL.4, REF.22 |
| Pub. Country;Japan |
| Language;Japanese |
| Abstract;This simple method is concerned with analysis of pesticides added to distilled water and atmosphere, in which they are adsorbed on the disk-format solid phase, extracted with acetone and then detected with a gas chromatography/mass spectrometry (GC/MS) with electron ionization (EI) after acetone is replaced by hexane. Under the analytical conditions, each calibration curve for standard pesticides is good linearity with correlation coefficient of 0.981-0.999 in the range from 0.2 .MU.g/l to 2 mg/l. High recovery was obtained for standard pesticides added to distilled water and reagent gas. (author abst.) |
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