Simple Spectrophotometric Flow Injection System with an In-valve Minicolumn for Enhancement during the Determination of Chromium(III) Using EDTA

Accession number;06A0028783
Title;Simple Spectrophotometric Flow Injection System with an In-valve Minicolumn for Enhancement during the Determination of Chromium(III) Using EDTA
Author; LAPANANTNOPPAKHUN SOMCHAI (Chiang Mai Univ., Chiang Mai, Tha) KASUWAS SUPHARPHORN (Chiang Mai Univ., Chiang Mai, Tha) GANRANOO LUCKSAGOON (Chiang Mai Univ., Chiang Mai, Tha) JAKMUNEE JAROON (Chiang Mai Univ., Chiang Mai, Tha) GRUDPAN KATE (Chiang Mai Univ., Chiang Mai, Tha)
Journal Title;Anal Sci
Journal Code:G0673B
ISSN:0910-6340
VOL.22;NO.1;PAGE.153-155(2006)
Figure&Table&Reference;FIG.1, TBL.2, REF.16
Pub. Country;Japan
Language;English
Abstract;A simple spectrophotometric flow injection (FI) procedure for the determination of Cr(III) using ethylenediaminetetraacetic acid (EDTA) was developed. An FI system with a column packed with Amberlite IR-120(H) was employed for sample pretreatment. This leads to the possibility of a single standard calibration. A linear calibration in a range of 10-27 .MU.g Cr(III) was obtained with a detection limit of 1 .MU.g Cr(III) and RSD of 2% (18 .MU.g Cr(III), n = 12). The proposed procedure was applied for determination of Cr(III) in leachate and dietary supplement samples. The results agreed with those obtained by the standard methods. (author abst.)
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