The Development of a Method for an Accurate Structural Analysis by Synchrotron X-ray Powder Diffraction

Accession number;06A0548455
Title;The Development of a Method for an Accurate Structural Analysis by Synchrotron X-ray Powder Diffraction
Author; NISHIBORI EIJI (Nagoya Univ., JPN)
Journal Title;Journal of the Crystallographic Society of Japan
Journal Code:G0232A
ISSN:0369-4585
VOL.48;NO.3;PAGE.216-223(2006)
Figure&Table&Reference;FIG.5, REF.27
Pub. Country;Japan
Language;Japanese
Abstract;The structural studies of powder diffraction using synchrotron radiation X-ray data have been described with some examples. The C2 entrapping structure of yttrium di-metallofullerene has been determined by Maximum Entropy method (MEM) combined with Rietveld refinement. The MEM analysis of Zn4Sb3, which is one of the most efficient thermoelectric materials, has been presented by both powder and single crystal method. The structure determination of a single-component palladium complex with extended TTF-type dithiolate ligands has also been described. (author abst.)